Parallel-Plate Viscometer: Symbolic Computations of Dynamic Viscosity
Housam Binous
Parallel-Plate Viscometer: Symbolic Computations of Dynamic Viscosity
Housam Binous
Housam Binous
Here, we determine the dynamic viscosity 𝜇 of a Newtonian and non-Newtonian fluids using a parallel-plate viscometer. In a parallel-plate viscometer, the fluid is sheared between two circular plates separated by a gap ℎ, with the top plate rotating at angular velocity ω. The shear rate varies linearly with radius: (r)= ω r/h, so the torque on the plate is obtained by integrating the local shear stress over the plate surface.For a Newtonian fluid: torque , and viscosity is directly .For a non-Newtonian power-law fluid (τ=κ*γ^n): 1- Measure torque 𝑇 at known ω, 𝑅, ℎ. 2- Use torque formula to solve for κ. We assume that the flow index 𝑛 is known or determined independently (by doing multiples measurements of torque 𝑇 at different angular velocities ω).3- Apply Rabinowitsch correction to get true wall shear rate (the apparent wall shear rate at the plate edge is corrected using the Rabinowitsch formula as follows : =[]).4- Compute true viscosity at wall: .Newtonian fluids: no correction needed (set ). Conversely, for Non-Newtonian fluids: Rabinowitsch correction ensures accurate viscosity measurement.A more general Rabinowitsch approach (valid for any non-Newtonian constitutive equation) given in Ref. 1 is the following:Note that a good temperature control is essential for the exact experimental determination of the dynamic viscosity.Nomenclature:μ (dynamic viscosity in Pa·s)ω (angular velocity of top plate in rad/s)h (gap between plates in m)R (radius of plates in m)r (radial coordinate in m)κ (consistency index)n (Power-law index)Reference:J. O. Wilkes, Fluid Mechanics for Chemical Engineers, 2nd edition, NJ: Prentice Hall, 2006.
γ
T=
πωμ
4
R
2h
μ=
2hTMeasured
πw
4
R
[]
γ
wall
(3+n)
4
γ
apparent
μ=κ
n-1
Rw(n+3)
4h
n=1
μ=
3TMeasuredh
2πw+
4
R
3
4
1
4
(ln(T))
(ln(w))
Newtonian fluid case
In[]:=
(*shearrateasafunctionofradius*)γdot=wr/h
Out[]=
rw
h
In[]:=
(*shearstress*)τ=μγdot
Out[]=
rwμ
h
In[]:=
(*differentialtorqueforanannularring*)dT=2τPir^2dr
Out[]=
2drπwμ
3
r
h
In[]:=
(*Totaltorque*)Ttotal=Integrate[dT/dr,{r,0,R}]
Out[]=
πwμ
4
R
2h
In[]:=
(*viscosityμ*)μExpr=μ/.Solve[Ttotal==TMeasured,μ][[1]]
Out[]=
2hTMeasured
πw
4
R
non-Newtonian fluid case
In[]:=
(*Non-NewtonianPower-LawFluid*)(*Shearstress:τ=κ*γ^n*)τPL=κ(γdot)^n
Out[]=
n
rw
h
In[]:=
(*Differentialtorque*)dTPL=2PiτPLr^2dr
Out[]=
2drπκ
2
r
n
rw
h
In[]:=
(*Totaltorque*)TtotalPowerLaw=Refine[Integrate[dTPL/dr,{r,0,R}],n>0]
Out[]=
2πκ
3
R
n
Rw
h
3+n
In[]:=
(*Apparentwallshearrate*)γdotApp=γdot/.r->R
Out[]=
Rw
h
In[]:=
(*Rabinowitschcorrection*)γdotTrue=((3+n)/4)γdotApp
Out[]=
(3+n)Rw
4h
In[]:=
(*Trueviscosityatwall*)ηWall=κ(γdotTrue/.r->R)^(n-1)
Out[]=
1-n
4
-1+n
(3+n)Rw
h
(*anotherderivationofTrueviscosityexpression*)
In[]:=
T[w_]:=Refine[Integrate[2Piκ(γdotTrue/.r->R)^nr^2,{r,0,R}],n>0]
In[]:=
T[w]//Simplify
Out[]=
1
3
1-2n
2
n
(3+n)
3
R
n
Rw
h
In[]:=
Simplify[D[T[w],w]]w/T[w]//Simplify
Out[]=
n
In[]:=
3T[w]h
2πw(3/4+1/4n)
4
R
Out[]=
1-n
4
-1+n
(3+n)
-1+n
Rw
h